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New Advances in Chemical Research, May 2021. The prevalence of solvent effects in heterogeneous catalysis in condensed media has motivated developing quantitative kinetic and spectroscopic. An article , which mentions Quality Control of 1,5-Diphenylpenta-1,4-dien-3-one, molecular formula is C17H14O. The compound – 1,5-Diphenylpenta-1,4-dien-3-one played an important role in people’s production and life., Quality Control of 1,5-Diphenylpenta-1,4-dien-3-one
Arylation of K2 with Mg(C6F3H2)Br in tetrahydrofuran-dioxane and subsequent addition of either benzonitrile or dibenzylideneacetone (dba) in diethyl ether leads to the formation of labile complexes or respectively.A number of -type complexes have been prepared by addition of the corresponding neutral ligand to chloroform solutions of .Proton, 19F, and 31P n.m.r. data for all the square-planar palladium(II) complexes have been collected and 31P-<1H> spectra show that they are the cis isomers.The complex reacts with NMe4Cl to give 2 and treatment of this with the appropriate alkali-metal salt (KBr, NaI, or KSCN) leads to 2 (X = Br, I, or SCN).The behaviour of the binuclear anions in the solvents acetone and dimethyl sulphoxide has been studied by 19F n.m.r. spectroscopy.The crystal structure of 2<(C6F3H2)2Pd(mu-SCN)(mu-NCS)Pd(C6F3H2)2> has been solved and refined to R = 0.040 based on 3384 observed reflections, confirming the existence of centrosymmetric binuclear anions where the Pd atoms have square-planar co-ordination .
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Reference：
Synthesis and Crystal Structure of a Chiral C3-Symmetric Oxygen Tripodal Ligand and Its Applications to Asymmetric Catalysis,
Chiral lanthanide(III) complexes of sulphur–nitrogen–oxygen ligand derived from aminothiourea and sodium D-camphor-β-sulfonate