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Two kinds of chiral segments, i.e. segment B-I (4) and segment B-II (5), which are potentially versatile building-blocks for construction of the right half of taxane-type diterpenoids, were synthesized from 3-methyl-2-cyclohexen-1-one (6) via optical resolution of the (2S,3S)-2,3-butanediol ketal derivatives (8, 15).Keywords – taxane-type diterpenoid; optical resolution with (2S,3S)-2,3-butanediol ketal; CD of cyclopropyl ketone; HPLC for optical resolution; ?-allylpalladium complex.
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Synthesis and Crystal Structure of a Chiral C3-Symmetric Oxygen Tripodal Ligand and Its Applications to Asymmetric Catalysis,
Chiral lanthanide(III) complexes of sulphur–nitrogen–oxygen ligand derived from aminothiourea and sodium D-camphor-β-sulfonate